In reply to Lankyman:
So funnily enough I just had this debate with myself re-proofing a gore-tex shell using TX.Direct that expired in 2020.
I haven't tested the jacket yet but it appears to have left a bunch of tiny clumps of residue clinging to the jacket. Not sure if that's related to the expiry or not and I don't use these products very often so not sure how common it is.
Currently re-washing to see if that clears it...